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3-Methoxybenzoic acid

  • Product Name: 3-Methoxybenzoic acid
  • CAS: 586-38-9
  • Purity:
  • Appearance: white to light yellow crystal powder

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Factory supply good quality 3-Methoxybenzoic acid 586-38-9 with stock

  • Molecular Formula:C8H8O3
  • Molecular Weight:152.15
  • Appearance/Colour:white to light yellow crystal powder 
  • Vapor Pressure:0.000303mmHg at 25°C 
  • Melting Point:105-107 °C(lit.) 
  • Refractive Index:1.4945 (estimate) 
  • Boiling Point:308 °C at 760 mmHg 
  • PKA:4.10(at 25℃) 
  • Flash Point:123.3 °C 
  • PSA：46.53000 
  • Density:1.207 g/cm3 
  • LogP:1.39340 

3-Methoxybenzoic acid(Cas 586-38-9) Usage

Safety Profile

Poison by intraperitoneal route.When heated to decomposition it emits acrid smoke andirritating fumes.

Purification Methods

Crystallise m-anisic acid from H2O (m 109o, 110.5o) or EtOH/water. The S-benzylisothiuronium salt has m 176o (from EtOH). [Beilstein 10 II 80, 10 III 244, 10 IV 316.]

General Description

3-Methoxybenzoic acid is an important intermediate in the synthesis of natural products.

InChI:InChI=1/C8H8O3/c1-11-7-4-2-3-6(5-7)8(9)10/h2-5H,1H3,(H,9,10)/p-1

586-38-9 Relevant articles

Mechanochemical Grignard Reactions with Gaseous CO2 and Sodium Methyl Carbonate**

Pfennig, Victoria S.,Villella, Romina C.,Nikodemus, Julia,Bolm, Carsten

supporting information, (2022/01/22)

A one-pot, three-step protocol for the p...

Aerobic oxidation of aldehydes to carboxylic acids catalyzed by recyclable ag/c3 n4 catalyst

Wu, Chaolong,Yao, Xiaoquan,Yu, Min,Zhou, Li,Zhu, Li

, p. 167 - 175 (2021/03/19)

The oxidation of aldehydes is an efficie...

One-Pot Direct Oxidation of Primary Amines to Carboxylic Acids through Tandem ortho-Naphthoquinone-Catalyzed and TBHP-Promoted Oxidation Sequence

Kim, Hun Young,Oh, Kyungsoo,Si, Tengda

supporting information, p. 18150 - 18155 (2021/12/09)

Biomimetic oxidation of primary amines t...

Selectively Upgrading Lignin Derivatives to Carboxylates through Electrochemical Oxidative C(OH)?C Bond Cleavage by a Mn-Doped Cobalt Oxyhydroxide Catalyst

Zhou, Hua,Li, Zhenhua,Xu, Si-Min,Lu, Lilin,Xu, Ming,Ji, Kaiyue,Ge, Ruixiang,Yan, Yifan,Ma, Lina,Kong, Xianggui,Zheng, Lirong,Duan, Haohong

supporting information, p. 8976 - 8982 (2021/03/16)

Oxidative cleavage of C(OH)?C bonds to a...

586-38-9 Process route

1-(3-methoxyphenyl)-3-(4-methoxyphenyl)propane-1,3-dione
252965-04-1

1-(3-methoxyphenyl)-3-(4-methoxyphenyl)propane-1,3-dione

furan-2,3,5(4H)-trione pyridine (1:1)

furan-2,3,5(4H)-trione pyridine (1:1)

3-Methoxybenzoic acid
586-38-9

3-Methoxybenzoic acid

4-methoxybenzoic acid
100-09-4

4-methoxybenzoic acid

Conditions
Conditions Yield
Das erhaltene Gemisch enthaelt 21-24prozent Anissaeure;
 
carbon monoxide
201230-82-2

carbon monoxide

methoxybenzene
100-66-3

methoxybenzene

3-Methoxybenzoic acid
586-38-9

3-Methoxybenzoic acid

4-methoxybenzoic acid
100-09-4

4-methoxybenzoic acid

Conditions
Conditions Yield
With palladium diacetate; dipotassium peroxodisulfate; In trifluoroacetic acid; for 20h; Yield given; Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
 

586-38-9 Upstream products

  • 186581-53-3
    186581-53-3

    diazomethane

  • 6304-89-8
    6304-89-8

    3-acetoxybenzoic acid

  • 67-56-1
    67-56-1

    methanol

  • 5434-20-8
    5434-20-8

    3-aminophthalic acid

586-38-9 Downstream products

  • 313402-19-6
    313402-19-6

    3-[4-(3-methoxy-benzoylamino)-phenyl]-coumarin

  • 94611-94-6
    94611-94-6

    3-methoxybenzoic acid anhydride

  • 1527-89-5
    1527-89-5

    3-methoxybenzonitrile

  • 75731-44-1
    75731-44-1

    4,3'-dimethoxybenzophenone

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