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With the increasing attention for green ...
A Ce-catalyzed strategy is developed to ...
A novel oxidative deoximation method was...
The 4, 4 ’ difluorobenzophenone and the ...
4,4'-difluorobenzhydryl alcohol
cyclohexanone
hexahydro-2H-oxepin-2-one
4,4'-Difluorobenzophenone
| Conditions | Yield |
|---|---|
|
4,4'-difluorobenzhydryl alcohol; cyclohexanone;
With
N-hydroxyphthalimide; 2,2'-azobis(isobutyronitrile); oxygen;
In
ethyl acetate;
at 75 ℃;
for 22h;
With
ammonium cerium (IV) nitrate; 1,1,1,3',3',3'-hexafluoro-propanol;
In
ethyl acetate;
at 45 ℃;
for 10h;
|
bis(methanesulfonyl)peroxide
4,4'-difluorodiphenylmethane
4,4'-difluorobenzhydryl alcohol
4,4'-Difluorobenzophenone
| Conditions | Yield |
|---|---|
|
bis(methanesulfonyl)peroxide; 4,4'-difluorodiphenylmethane;
With
trimethylsilyl acetate; copper (I) acetate;
In
dichloromethane;
at 23 ℃;
for 12h;
Inert atmosphere;
With
sodium methylate;
In
methanol;
at 23 ℃;
for 8h;
|
34% 9% |
tetrachloromethane
fluorobenzene
phosgene
dichloro-bis-(4-fluoro-phenyl)-methane
1,1,2,2-tetrakis-(4-fluorophenyl)-ethane-1,2-diol
ethyl 3,3-bis(4-fluorophenyl)-3-hydroxypropanoate
1,1-bis-(4-fluoro-phenyl)-ethanol
tris-(4-fluoro-phenyl)-ethene
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